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Information card for entry 4064141
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Coordinates | 4064141.cif |
---|---|
Original paper (by DOI) | HTML |
Common name | [(tBuPCO)Pd]2(?-CO3) |
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Chemical name | (9) |
Formula | C35 H56 O5 P2 Pd2 |
Calculated formula | C35 H56 O5 P2 Pd2 |
SMILES | c12c(cccc1COC)C[P](C(C)(C)C)(C(C)(C)C)[Pd]12[O]=C(O1)O[Pd]12c3c(cccc3C[O]1C)C[P]2(C(C)(C)C)C(C)(C)C |
Title of publication | Syntheses and Characterization of Palladium Complexes with a Hemilabile “PCO” Pincer Ligand |
Authors of publication | Fulmer, Gregory R.; Kaminsky, Werner; Kemp, Richard A.; Goldberg, Karen I. |
Journal of publication | Organometallics |
Year of publication | 2011 |
Journal volume | 30 |
Journal issue | 6 |
Pages of publication | 1627 |
a | 52.6 ± 0.003 Å |
b | 11.1482 ± 0.0006 Å |
c | 12.4825 ± 0.0006 Å |
α | 90° |
β | 95.827 ± 0.006° |
γ | 90° |
Cell volume | 7281.9 ± 0.7 Å3 |
Cell temperature | 110 ± 2 K |
Ambient diffraction temperature | 110 ± 2 K |
Number of distinct elements | 5 |
Space group number | 15 |
Hermann-Mauguin space group symbol | C 1 2/c 1 |
Hall space group symbol | -C 2yc |
Residual factor for all reflections | 0.0758 |
Residual factor for significantly intense reflections | 0.0677 |
Weighted residual factors for significantly intense reflections | 0.1392 |
Weighted residual factors for all reflections included in the refinement | 0.143 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.237 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/4064141.html
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