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Information card for entry 4064149
Preview
Coordinates | 4064149.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C61 H60 Cl2 F24 Ir2 N6 P4 |
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Calculated formula | C61 H60 Cl2 F24 Ir2 N6 P4 |
Title of publication | Open-Shell Organometallic [MII(dbcot(bislutidylamine)]2+Complexes (M = Rh, Ir): Unexpected Base-Assisted Reduction of the Metal Instead of Amine Ligand Deprotonation |
Authors of publication | Dzik, Wojciech I.; Fuente Arruga, Luis; Siegler, Maxime A.; Spek, Anthony L.; Reek, Joost N. H.; de Bruin, Bas |
Journal of publication | Organometallics |
Year of publication | 2011 |
Journal volume | 30 |
Journal issue | 7 |
Pages of publication | 1902 |
a | 21.5483 ± 0.0009 Å |
b | 16.7416 ± 0.0007 Å |
c | 20.9573 ± 0.0008 Å |
α | 90° |
β | 110.52 ± 0.002° |
γ | 90° |
Cell volume | 7080.7 ± 0.5 Å3 |
Cell temperature | 110 ± 2 K |
Ambient diffraction temperature | 110 ± 2 K |
Number of distinct elements | 7 |
Space group number | 14 |
Hermann-Mauguin space group symbol | P 1 21/c 1 |
Hall space group symbol | -P 2ybc |
Residual factor for all reflections | 0.0517 |
Residual factor for significantly intense reflections | 0.0292 |
Weighted residual factors for significantly intense reflections | 0.0702 |
Weighted residual factors for all reflections included in the refinement | 0.0759 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.101 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/4064149.html
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