Information card for entry 4064214

Structure parameters

• Formula: C32 H44 Cl O8 Os P Sn
• Calculated formula: C32 H44 Cl O8 Os P Sn
• SMILES: [Os]12345(Cl)([Sn](C(=C)C(=O)OC)(C(=C)C(=O)OC)C(=C)C(=O)OC)([c]6([cH]1[cH]2[c]3([cH]4[cH]56)C)C(C)C)[P](OCC)(OCC)c1ccccc1
• Title of publication: Preparation of Half-Sandwich Stannyl Complexes of Osmium(II)
• Authors of publication: Albertin, Gabriele; Antoniutti, Stefano; Castro, Jesús
• Journal of publication: Organometallics
• Year of publication: 2011
• Journal volume: 30
• Journal issue: 7
• Pages of publication: 1914
• a: 10.0128 ± 0.0008 Å
• b: 11.0162 ± 0.0009 Å
• c: 18.3313 ± 0.0014 Å
• α: 77.644 ± 0.001°
• β: 87.243 ± 0.002°
• γ: 81.271 ± 0.001°
• Cell volume: 1952 ± 0.3 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0553
• Residual factor for significantly intense reflections: 0.0468
• Weighted residual factors for significantly intense reflections: 0.1458
• Weighted residual factors for all reflections included in the refinement: 0.1549
• Goodness-of-fit parameter for all reflections included in the refinement: 1.08
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No