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Information card for entry 4064222
Preview
Coordinates | 4064222.cif |
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Original paper (by DOI) | HTML |
Formula | C64.25 H48.5 B Cl0.5 F24 Mn N2 O5 |
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Calculated formula | C64 H48 B F24 Mn N2 O5 |
Title of publication | Neutral and Cationic Mono- and Bis-N-heterocyclic Carbene Complexes Derived From Manganese and Rhenium Carbonyl Precursors |
Authors of publication | Martin, Thomas A.; Ellul, Charles E.; Mahon, Mary F.; Warren, Mark E.; Allan, David; Whittlesey, Michael K. |
Journal of publication | Organometallics |
Year of publication | 2011 |
Journal volume | 30 |
Journal issue | 8 |
Pages of publication | 2200 |
a | 13.551 ± 0.0002 Å |
b | 15.538 ± 0.0002 Å |
c | 17.02 ± 0.0002 Å |
α | 101.05 ± 0.001° |
β | 104.266 ± 0.001° |
γ | 99.296 ± 0.001° |
Cell volume | 3325.64 ± 0.08 Å3 |
Cell temperature | 150 ± 2 K |
Ambient diffraction temperature | 150 ± 2 K |
Number of distinct elements | 8 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.076 |
Residual factor for significantly intense reflections | 0.0593 |
Weighted residual factors for significantly intense reflections | 0.1507 |
Weighted residual factors for all reflections included in the refinement | 0.1602 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.055 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
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The link is: https://www.crystallography.net/4064222.html
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