Information card for entry 4064291

Structure parameters

• Formula: C31 H82 Ge2 Mg O2 Si6
• Calculated formula: C31 H82 Ge2 Mg O2 Si6
• Title of publication: Novel Stable Silyl, Germyl, and Stannyl Germanium(II) Compounds Containing an Amidinato Ligand
• Authors of publication: Matioszek, Dimitri; Katir, Nadia; Ladeira, Sonia; Castel, Annie
• Journal of publication: Organometallics
• Year of publication: 2011
• Journal volume: 30
• Journal issue: 8
• Pages of publication: 2230
• a: 18.7428 ± 0.0003 Å
• b: 15.5144 ± 0.0003 Å
• c: 18.7568 ± 0.0003 Å
• α: 90°
• β: 115.691 ± 0.001°
• γ: 90°
• Cell volume: 4914.99 ± 0.15 ų
• Cell temperature: 193 ± 2 K
• Ambient diffraction temperature: 193 ± 2 K
• Number of distinct elements: 6
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.053
• Residual factor for significantly intense reflections: 0.0331
• Weighted residual factors for significantly intense reflections: 0.0846
• Weighted residual factors for all reflections included in the refinement: 0.0971
• Goodness-of-fit parameter for all reflections included in the refinement: 1.036
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No