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Information card for entry 4064313
Preview
Coordinates | 4064313.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C17 H26 Si3 |
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Calculated formula | C17 H26 Si3 |
SMILES | [Si](C)(c1ccccc1)(C#C[Si](C)(C)C)C#C[Si](C)(C)C |
Title of publication | Silylative Coupling of Terminal Alkynes with Iodosilanes: New Catalytic Activation of sp-Hybridized Carbon−Hydrogen Bonds |
Authors of publication | Kownacki, Ireneusz; Marciniec, Bogdan; Dudziec, Beata; Kubicki, Maciej |
Journal of publication | Organometallics |
Year of publication | 2011 |
Journal volume | 30 |
Journal issue | 9 |
Pages of publication | 2539 |
a | 12.732 ± 0.002 Å |
b | 13.341 ± 0.002 Å |
c | 14.722 ± 0.003 Å |
α | 113.47 ± 0.01° |
β | 98.63 ± 0.02° |
γ | 104.93 ± 0.02° |
Cell volume | 2124.4 ± 0.8 Å3 |
Cell temperature | 295 ± 2 K |
Ambient diffraction temperature | 295 ± 2 K |
Number of distinct elements | 3 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.0577 |
Residual factor for significantly intense reflections | 0.052 |
Weighted residual factors for significantly intense reflections | 0.1163 |
Weighted residual factors for all reflections included in the refinement | 0.1194 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.128 |
Diffraction radiation wavelength | 1.54178 Å |
Diffraction radiation type | CuKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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The link is: https://www.crystallography.net/4064313.html
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