Information card for entry 4064327

Structure parameters

• Formula: C117 H132 N10 O3 Si Sm4
• Calculated formula: C117 H132 N10 O3 Si Sm4
• Title of publication: Lanthanide(II)−Alkali Sandwich Complexes with Cation−Arene π Interactions: Synthesis, Structure, and Solvent-Mediated Redox Transformations
• Authors of publication: Pan, Cheng-Ling; Chen, Wan; Song, Jiangfeng
• Journal of publication: Organometallics
• Year of publication: 2011
• Journal volume: 30
• Journal issue: 8
• Pages of publication: 2252
• a: 14.1516 ± 0.0012 Å
• b: 17.8697 ± 0.0015 Å
• c: 20.9102 ± 0.0019 Å
• α: 86.765 ± 0.002°
• β: 87.113 ± 0.002°
• γ: 82.227 ± 0.001°
• Cell volume: 5226.1 ± 0.8 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 273 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0882
• Residual factor for significantly intense reflections: 0.0544
• Weighted residual factors for significantly intense reflections: 0.1308
• Weighted residual factors for all reflections included in the refinement: 0.1562
• Goodness-of-fit parameter for all reflections included in the refinement: 1.034
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No