Information card for entry 4064429

Structure parameters

• Formula: C56 H78 Al2 Cl4 Cr2 N4 P4
• Calculated formula: C56 H78 Al2 Cl4 Cr2 N4 P4
• Title of publication: Heterobimetallic Al−Cl−Cr Intermediates with Relevance to the Selective Catalytic Ethene Trimerization Systems Consisting of CrCl3(THF)3, the Aminophosphorus Ligands Ph2PN(R)P(Ph)N(R)H, and Triethylaluminum
• Authors of publication: Peitz, Stephan; Peulecke, Normen; Müller, Bernd H.; Spannenberg, Anke; Drexler, Hans-Joachim; Rosenthal, Uwe; Al-Hazmi, Mohammed H.; Al-Eidan, Khalid E.; Wöhl, Anina; Müller, Wolfgang
• Journal of publication: Organometallics
• Year of publication: 2011
• Journal volume: 30
• Journal issue: 8
• Pages of publication: 2364
• a: 11.4748 ± 0.0005 Å
• b: 15.2374 ± 0.0004 Å
• c: 17.9504 ± 0.0007 Å
• α: 90°
• β: 98.103 ± 0.003°
• γ: 90°
• Cell volume: 3107.2 ± 0.2 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0851
• Residual factor for significantly intense reflections: 0.0534
• Weighted residual factors for significantly intense reflections: 0.1315
• Weighted residual factors for all reflections included in the refinement: 0.1407
• Goodness-of-fit parameter for all reflections included in the refinement: 0.946
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No