Crystallography Open Database

Information card for entry 4064484

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Coordinates	4064484.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C28 H44 P2 Ru Zr
Calculated formula	C28 H44 P2 Ru Zr
Title of publication	Synthesis of Group IV (Zr, Hf)−Group VIII (Fe, Ru) Heterobimetallic Complexes Bearing Metallocenyl Diphosphine Moieties and Their Application to Catalytic Dehydrogenation of Amine−Boranes
Authors of publication	Miyazaki, Takamasa; Tanabe, Yoshiaki; Yuki, Masahiro; Miyake, Yoshihiro; Nishibayashi, Yoshiaki
Journal of publication	Organometallics
Year of publication	2011
Journal volume	30
Journal issue	8
Pages of publication	2394
a	25.306 ± 0.0012 Å
b	10.2628 ± 0.0004 Å
c	20.6056 ± 0.0008 Å
α	90°
β	91.944 ± 0.0016°
γ	90°
Cell volume	5348.4 ± 0.4 Å³
Cell temperature	173.1 K
Ambient diffraction temperature	173.1 K
Number of distinct elements	5
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for significantly intense reflections	0.0617
Weighted residual factors for all reflections included in the refinement	0.1599
Goodness-of-fit parameter for all reflections included in the refinement	1
Diffraction radiation wavelength	0.71075 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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