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Information card for entry 4064486
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Jmol._Canvas2D (Jmol) "jmolApplet0"[x]
Coordinates | 4064486.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C22 H29 N Si2 |
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Calculated formula | C22 H29 N Si2 |
SMILES | [Si]1([C@H]([C@H]([SiH](C)C)c2n(c3c(c12)cccc3)C)c1ccc(cc1)C)(C)C.[Si]1([C@@H]([C@@H]([SiH](C)C)c2n(c3c(c12)cccc3)C)c1ccc(cc1)C)(C)C |
Title of publication | 2-Vinylindoles As the Four-Atom Component in a Catalytic [4+1] Cycloaddition with a Silylene-Palladium Species Generated from (Aminosilyl)boronic Ester |
Authors of publication | Masuda, Kohei; Ohmura, Toshimichi; Suginome, Michinori |
Journal of publication | Organometallics |
Year of publication | 2011 |
Journal volume | 30 |
Journal issue | 6 |
Pages of publication | 1322 |
a | 14.5564 ± 0.0005 Å |
b | 8.1265 ± 0.0002 Å |
c | 19.5917 ± 0.0006 Å |
α | 90° |
β | 112.229 ± 0.001° |
γ | 90° |
Cell volume | 2145.32 ± 0.11 Å3 |
Cell temperature | 100 ± 2 K |
Ambient diffraction temperature | 100 ± 2 K |
Number of distinct elements | 4 |
Space group number | 14 |
Hermann-Mauguin space group symbol | P 1 21/a 1 |
Hall space group symbol | -P 2yab |
Residual factor for all reflections | 0.0451 |
Residual factor for significantly intense reflections | 0.0349 |
Weighted residual factors for significantly intense reflections | 0.0882 |
Weighted residual factors for all reflections included in the refinement | 0.094 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.039 |
Diffraction radiation wavelength | 0.71075 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/4064486.html
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structural data.