Information card for entry 4064491
| Formula |
C66.5 H82.5 O4 Ta |
| Calculated formula |
C66.5 H82.5 O4 Ta |
| Title of publication |
Synthesis of Novel Tantalacalixarene Complexes: First Example of Intramolecular CH Activation of Monodepleted Aromatic Ring |
| Authors of publication |
Espinas, Jeff; Pelletier, Jérémie; Jeanneau, Erwan; Darbost, Ulrich; Szeto, Kai C.; Lucas, Christine; Thivolle-Cazat, Jean; Duchamp, Christian; Henriques, Natali; Bouchu, Denis; Basset, Jean-Marie; Chermette, Henry; Bonnamour, Isabelle; Taoufik, Mostafa |
| Journal of publication |
Organometallics |
| Year of publication |
2011 |
| Journal volume |
30 |
| Journal issue |
13 |
| Pages of publication |
3512 |
| a |
14.653 ± 0.005 Å |
| b |
19.076 ± 0.005 Å |
| c |
21.946 ± 0.005 Å |
| α |
90° |
| β |
105.974 ± 0.005° |
| γ |
90° |
| Cell volume |
5897 ± 3 Å3 |
| Cell temperature |
150 K |
| Ambient diffraction temperature |
150 K |
| Number of distinct elements |
4 |
| Space group number |
14 |
| Hermann-Mauguin space group symbol |
P 1 21/c 1 |
| Hall space group symbol |
-P 2ybc |
| Residual factor for all reflections |
0.089 |
| Residual factor for significantly intense reflections |
0.0332 |
| Weighted residual factors for all reflections |
0.0763 |
| Weighted residual factors for significantly intense reflections |
0.0256 |
| Weighted residual factors for all reflections included in the refinement |
0.0236 |
| Goodness-of-fit parameter for all reflections included in the refinement |
1.1336 |
| Diffraction radiation wavelength |
0.71069 Å |
| Diffraction radiation type |
MoKα |
| Has coordinates |
Yes |
| Has disorder |
Yes |
| Has Fobs |
No |
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https://www.crystallography.net/4064491.html
