Information card for entry 4064517

Structure parameters

• Formula: C36 H56 P4 Pd2 Si2
• Calculated formula: C36 H56 P4 Pd2 Si2
• SMILES: c1c(cccc1)[Si]1([Pd]([P](C)(C)C)([P](C)(C)C)[Si](c2ccccc2)(c2ccccc2)[Pd]1([P](C)(C)C)[P](C)(C)C)c1ccccc1
• Title of publication: Dinuclear Palladium and Platinum Complexes with Bridging Silylene Ligands. Preparation Using (Aminosilyl)boronic Ester as the Ligand Precursor and Their Reactions with Alkynes
• Authors of publication: Tanabe, Makoto; Jiang, Jian; Yamazawa, Hideto; Osakada, Kohtaro; Ohmura, Toshimichi; Suginome, Michinori
• Journal of publication: Organometallics
• Year of publication: 2011
• Journal volume: 30
• Journal issue: 15
• Pages of publication: 3981
• a: 9.609 ± 0.004 Å
• b: 10.751 ± 0.005 Å
• c: 11.421 ± 0.005 Å
• α: 98.7843 ± 0.0013°
• β: 111.692 ± 0.004°
• γ: 106.126 ± 0.007°
• Cell volume: 1009.2 ± 0.8 ų
• Cell temperature: 113.1 K
• Ambient diffraction temperature: 113 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0404
• Residual factor for significantly intense reflections: 0.0316
• Weighted residual factors for significantly intense reflections: 0.0828
• Weighted residual factors for all reflections included in the refinement: 0.0861
• Goodness-of-fit parameter for all reflections included in the refinement: 0.989
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No