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Information card for entry 4064529
Preview
Coordinates | 4064529.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C30 H48 Al Cl N Ni P |
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Calculated formula | C30 H48 Al Cl N Ni P |
SMILES | [Ni]12([Cl][Al]([N]1=C1C(C2)Cc2c1cccc2)(C)C)[P](C1CCCCC1)(C1CCCCC1)C1CCCCC1 |
Title of publication | Intramolecular Oxidative Cyclization of Alkenes and Nitriles with Nickel(0) |
Authors of publication | Ohashi, Masato; Ikawa, Masashi; Ogoshi, Sensuke |
Journal of publication | Organometallics |
Year of publication | 2011 |
Journal volume | 30 |
Journal issue | 10 |
Pages of publication | 2765 |
a | 16.6868 ± 0.0013 Å |
b | 10.2681 ± 0.0008 Å |
c | 18.9795 ± 0.0017 Å |
α | 90° |
β | 113.851 ± 0.002° |
γ | 90° |
Cell volume | 2974.3 ± 0.4 Å3 |
Cell temperature | 296 ± 2 K |
Ambient diffraction temperature | 296 ± 2 K |
Number of distinct elements | 7 |
Space group number | 14 |
Hermann-Mauguin space group symbol | P 1 21/c 1 |
Hall space group symbol | -P 2ybc |
Residual factor for all reflections | 0.1142 |
Residual factor for significantly intense reflections | 0.0641 |
Weighted residual factors for significantly intense reflections | 0.1579 |
Weighted residual factors for all reflections included in the refinement | 0.2034 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.122 |
Diffraction radiation wavelength | 0.71075 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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The link is: https://www.crystallography.net/4064529.html
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