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Information card for entry 4064732
Preview
Coordinates | 4064732.cif |
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Original paper (by DOI) | HTML |
Formula | C53 H49 Cl9 P4 Pd2 |
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Calculated formula | C53 H45 Cl9 P4 Pd2 |
Title of publication | The First Carbodiphosphorane Complex with Two Palladium Centers Attached to the CDP Carbon: Assembly of a Single-Stranded di-Pd Helicate by the PCP Pincer ligand C(dppm)2 |
Authors of publication | Reitsamer, Christian; Schuh, Walter; Kopacka, Holger; Wurst, Klaus; Ellmerer, Ernst P.; Peringer, Paul |
Journal of publication | Organometallics |
Year of publication | 2011 |
Journal volume | 30 |
Journal issue | 15 |
Pages of publication | 4220 |
a | 12.9599 ± 0.0004 Å |
b | 16.8199 ± 0.0005 Å |
c | 13.9015 ± 0.0006 Å |
α | 90° |
β | 104.255 ± 0.002° |
γ | 90° |
Cell volume | 2937 ± 0.18 Å3 |
Cell temperature | 233 ± 2 K |
Ambient diffraction temperature | 233 ± 2 K |
Number of distinct elements | 5 |
Space group number | 4 |
Hermann-Mauguin space group symbol | P 1 21 1 |
Hall space group symbol | P 2yb |
Residual factor for all reflections | 0.0691 |
Residual factor for significantly intense reflections | 0.0555 |
Weighted residual factors for significantly intense reflections | 0.1382 |
Weighted residual factors for all reflections included in the refinement | 0.1469 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.051 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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The link is: https://www.crystallography.net/4064732.html
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