Information card for entry 4064734

Structure parameters

• Formula: C14 H23 O7 P Si2 W
• Calculated formula: C14 H23 O7 P Si2 W
• SMILES: C(=O)(C)O[P@@H](C([Si](C)(C)C)[Si](C)(C)C)[W](C#[O])(C#[O])(C#[O])(C#[O])C#[O]
• Title of publication: Generation and Decomposition of Li/OR Phosphinidenoid Complexes
• Authors of publication: Duan, Lili; Schnakenburg, Gregor; Streubel, Rainer
• Journal of publication: Organometallics
• Year of publication: 2011
• Journal volume: 30
• Journal issue: 12
• Pages of publication: 3246
• a: 9.1768 ± 0.0003 Å
• b: 16.9657 ± 0.0006 Å
• c: 27.8831 ± 0.0011 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 4341.1 ± 0.3 ų
• Cell temperature: 123 ± 2 K
• Ambient diffraction temperature: 123 ± 2 K
• Number of distinct elements: 6
• Space group number: 20
• Hermann-Mauguin space group symbol: C 2 2 21
• Hall space group symbol: C 2c 2
• Residual factor for all reflections: 0.0214
• Residual factor for significantly intense reflections: 0.0201
• Weighted residual factors for significantly intense reflections: 0.0438
• Weighted residual factors for all reflections included in the refinement: 0.0442
• Goodness-of-fit parameter for all reflections included in the refinement: 1.014
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No