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Information card for entry 4064832
Preview
Coordinates | 4064832.cif |
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Original paper (by DOI) | HTML |
Formula | C161 H117 Cl23 O4 P8 Pd4 |
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Calculated formula | C161 H117 Cl23 O4 P8 Pd4 |
Title of publication | κ1- and κ2-Complexes of Fluorenylidene‒Allenyl Phosphines and Phosphine Oxides with Palladium Chloride and Iron Carbonyl: Displacement of Trimethylsilyl by Diphenylphosphino via a Stabilized Carbanion |
Authors of publication | Milosevic, Sandra; Banide, Emilie V.; Müller-Bunz, Helge; Gilheany, Declan G.; McGlinchey, Michael J. |
Journal of publication | Organometallics |
Year of publication | 2011 |
Journal volume | 30 |
Journal issue | 14 |
Pages of publication | 3804 |
a | 10.4539 ± 0.0003 Å |
b | 12.5942 ± 0.0003 Å |
c | 29.1459 ± 0.0007 Å |
α | 84.129 ± 0.002° |
β | 87.199 ± 0.002° |
γ | 81.094 ± 0.002° |
Cell volume | 3769.03 ± 0.17 Å3 |
Cell temperature | 100 ± 2 K |
Ambient diffraction temperature | 100 ± 2 K |
Number of distinct elements | 6 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.0385 |
Residual factor for significantly intense reflections | 0.031 |
Weighted residual factors for significantly intense reflections | 0.0805 |
Weighted residual factors for all reflections included in the refinement | 0.083 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.064 |
Diffraction radiation wavelength | 1.54184 Å |
Diffraction radiation type | CuKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/4064832.html
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