Information card for entry 4064944

Structure parameters

• Formula: C18 H41 Cl N2 Ni P2
• Calculated formula: C18 H41 Cl N2 Ni P2
• Title of publication: Nickel(II) and Palladium(II) Bis-Aminophosphine Pincer Complexes
• Authors of publication: Gwynne, Erin A.; Stephan, Douglas W.
• Journal of publication: Organometallics
• Year of publication: 2011
• Journal volume: 30
• Journal issue: 15
• Pages of publication: 4128
• a: 8.0239 ± 0.0011 Å
• b: 14.246 ± 0.002 Å
• c: 10.4439 ± 0.0014 Å
• α: 90°
• β: 99.861 ± 0.009°
• γ: 90°
• Cell volume: 1176.2 ± 0.3 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 6
• Space group number: 11
• Hermann-Mauguin space group symbol: P 1 21/m 1
• Hall space group symbol: -P 2yb
• Residual factor for all reflections: 0.0923
• Residual factor for significantly intense reflections: 0.0546
• Weighted residual factors for significantly intense reflections: 0.1362
• Weighted residual factors for all reflections included in the refinement: 0.155
• Goodness-of-fit parameter for all reflections included in the refinement: 1.074
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No