Crystallography Open Database

Information card for entry 4065010

Preview

Coordinates	4065010.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C37.5 H40 B Cl F Sb
Calculated formula	C37.5 H40 B Cl F Sb
Title of publication	Fluoride Anion Chelation by a Bidentate Stibonium‒Borane Lewis Acid
Authors of publication	Wade, Casey R.; Gabbaï, François P.
Journal of publication	Organometallics
Year of publication	2011
Journal volume	30
Journal issue	17
Pages of publication	4479
a	9.0227 ± 0.0002 Å
b	16.336 ± 0.0004 Å
c	22.9463 ± 0.0005 Å
α	90°
β	101.691 ± 0.001°
γ	90°
Cell volume	3312 ± 0.13 Å³
Cell temperature	110 ± 2 K
Ambient diffraction temperature	110 ± 2 K
Number of distinct elements	6
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.0614
Residual factor for significantly intense reflections	0.0456
Weighted residual factors for significantly intense reflections	0.1268
Weighted residual factors for all reflections included in the refinement	0.1377
Goodness-of-fit parameter for all reflections included in the refinement	1.015
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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