Information card for entry 4065131

Structure parameters

• Common name: [PtH(GeH2Trip)(dcpe)_ 3 (C4H8O)
• Chemical name: [PtH(GeH2Trip)(dcpe)_ 3 (C4H8O)
• Formula: C58 H88 Ge O3 P2 Pd
• Calculated formula: C58 H88 Ge O3 P2 Pd
• Title of publication: Palladium(II) Hydrido Complexes Having a Primary Silyl or Germyl Ligand: Synthesis, Crystal Structures, and Dynamic Behavior
• Authors of publication: Nakata, Norio; Fukazawa, Shun; Kato, Nanami; Ishii, Akihiko
• Journal of publication: Organometallics
• Year of publication: 2011
• Journal volume: 30
• Journal issue: 17
• Pages of publication: 4490
• a: 16.4583 ± 0.0011 Å
• b: 19.8712 ± 0.0013 Å
• c: 17.2632 ± 0.0012 Å
• α: 90°
• β: 105.531 ± 0.001°
• γ: 90°
• Cell volume: 5439.7 ± 0.6 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0533
• Residual factor for significantly intense reflections: 0.045
• Weighted residual factors for significantly intense reflections: 0.111
• Weighted residual factors for all reflections included in the refinement: 0.1166
• Goodness-of-fit parameter for all reflections included in the refinement: 1.04
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No