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Information card for entry 4065145
Preview
Coordinates | 4065145.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C22.85 H41 B2 Cl1.7 F4 N6 O0.15 Os P |
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Calculated formula | C22.85 H41 B2 Cl1.7 F4 N6 O0.15 Os P |
Title of publication | Reactions of an Osmium Bis(dihydrogen) Complex under Ethylene: Phosphine Addition to a C‒C Double Bond and C‒H Bond Activation of Fluoroarenes |
Authors of publication | Bajo, Sonia; Esteruelas, Miguel A.; López, Ana M.; Oñate, Enrique |
Journal of publication | Organometallics |
Year of publication | 2011 |
Journal volume | 30 |
Journal issue | 21 |
Pages of publication | 5710 |
a | 8.7811 ± 0.0004 Å |
b | 18.3167 ± 0.0008 Å |
c | 18.741 ± 0.0009 Å |
α | 90° |
β | 101.68 ± 0.001° |
γ | 90° |
Cell volume | 2951.9 ± 0.2 Å3 |
Cell temperature | 100 ± 2 K |
Ambient diffraction temperature | 100 ± 2 K |
Number of distinct elements | 9 |
Space group number | 14 |
Hermann-Mauguin space group symbol | P 1 21/n 1 |
Hall space group symbol | -P 2yn |
Residual factor for all reflections | 0.0385 |
Residual factor for significantly intense reflections | 0.0294 |
Weighted residual factors for significantly intense reflections | 0.0749 |
Weighted residual factors for all reflections included in the refinement | 0.0855 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.105 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/4065145.html
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