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Information card for entry 4065155
Preview
Coordinates | 4065155.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C105 H24 Cl2 O20 Os6 P2 |
---|---|
Calculated formula | C105 H24 Cl2 O20 Os6 P2 |
SMILES | C(#[O])[Os]12(C#[O])(C#[O])[P](c3ccccc3)(c3ccccc3)C34C5=C6c7c8C3C3C9c%10c4c4[C]%115=[C]5(c%12c6c6c7c7c%13c%14C%15=C%16C%17(C=3c8c7%15)c3c7c8c%15c(c%10c%10c4c4c%18c%19c%20c(c%12c%12c6c%13c6c%12c%20c%12c%13c6c%14[C]6(c%13c8c(c%19%12)c%15c%10%18)=[C]%167[Os]76(C#[O])(C#[O])(C#[O])[Os](C#[O])(C#[O])(C#[O])([P]%17(c6ccccc6)c6ccccc6)[Os]7(C#[O])(C#[O])(C#[O])C#[O])c54)c93)[Os]1%11(C#[O])(C#[O])(C#[O])[Os]2(C#[O])(C#[O])(C#[O])C#[O].C(Cl)Cl |
Title of publication | Synthesis of the Diphosphino‒Fullerene 1,2,4,15-(PPh2)2(H)2C60and Its Complexation with Triosmium Carbonyl Clusters |
Authors of publication | Wu, Yi-Ying; Yeh, Wen-Yann |
Journal of publication | Organometallics |
Year of publication | 2011 |
Journal volume | 30 |
Journal issue | 17 |
Pages of publication | 4792 |
a | 15.3318 ± 0.0005 Å |
b | 17.5972 ± 0.0005 Å |
c | 19.1755 ± 0.0006 Å |
α | 69.011 ± 0.002° |
β | 88.52 ± 0.002° |
γ | 80.585 ± 0.002° |
Cell volume | 4762.1 ± 0.3 Å3 |
Cell temperature | 200 ± 2 K |
Ambient diffraction temperature | 200 ± 2 K |
Number of distinct elements | 6 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.042 |
Residual factor for significantly intense reflections | 0.0334 |
Weighted residual factors for significantly intense reflections | 0.1014 |
Weighted residual factors for all reflections included in the refinement | 0.1054 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.068 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/4065155.html
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