Information card for entry 4065521

Structure parameters

• Formula: C50 H79 N3 Si2 Zr
• Calculated formula: C50.22 H88 N3 Si2 Zr
• Title of publication: Synthesis of Bis(amino)pyridines by the Stepwise Alkylation of Bis(imino)pyridines: An Unexpected and Selective Alkylation of the Aminoiminopyridine by AlMe3
• Authors of publication: Tay, Boon-Ying; Wang, Cun; Chia, Sze-Chen; Stubbs, Ludger P.; Wong, Pui-Kwan; van Meurs, Martin
• Journal of publication: Organometallics
• Year of publication: 2011
• Journal volume: 30
• Journal issue: 21
• Pages of publication: 6028
• a: 24.951 ± 0.01 Å
• b: 13.912 ± 0.005 Å
• c: 14.168 ± 0.006 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 4918 ± 3 ų
• Cell temperature: 110.1 K
• Number of distinct elements: 5
• Space group number: 62
• Hermann-Mauguin space group symbol: P n m a
• Hall space group symbol: -P 2ac 2n
• Residual factor for significantly intense reflections: 0.082
• Weighted residual factors for all reflections included in the refinement: 0.08
• Goodness-of-fit parameter for all reflections included in the refinement: 3.807
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No