Information card for entry 4065523

Structure parameters

• Formula: C30 H46 O2 Os2 Ru
• Calculated formula: C30 H45 O2 Os2.01 Ru0.99
• Title of publication: Heterometallic Effects in Nitrogen‒Hydrogen Bond Cleavage by Trinuclear Mixed-Metal Polyhydrido Clusters Containing Ruthenium and Osmium
• Authors of publication: Kameo, Hajime; Nakajima, Yumiko; Namura, Kyo; Suzuki, Hiroharu
• Journal of publication: Organometallics
• Year of publication: 2011
• Journal volume: 30
• Journal issue: 24
• Pages of publication: 6703
• a: 18.451 ± 0.004 Å
• b: 18.451 ± 0.004 Å
• c: 15.731 ± 0.004 Å
• α: 90°
• β: 90°
• γ: 120°
• Cell volume: 4638 ± 1.8 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 5
• Space group number: 148
• Hermann-Mauguin space group symbol: R -3 :H
• Hall space group symbol: -R 3
• Residual factor for all reflections: 0.0266
• Residual factor for significantly intense reflections: 0.024
• Weighted residual factors for significantly intense reflections: 0.0627
• Weighted residual factors for all reflections included in the refinement: 0.0639
• Goodness-of-fit parameter for all reflections included in the refinement: 1.104
• Diffraction radiation wavelength: 0.71069 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No