Crystallography Open Database

Information card for entry 4065525

Preview

Coordinates	4065525.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C30 H49 N Os Ru2
Calculated formula	C30 H48 N Os0.99 Ru1.98
Title of publication	Heterometallic Effects in Nitrogen‒Hydrogen Bond Cleavage by Trinuclear Mixed-Metal Polyhydrido Clusters Containing Ruthenium and Osmium
Authors of publication	Kameo, Hajime; Nakajima, Yumiko; Namura, Kyo; Suzuki, Hiroharu
Journal of publication	Organometallics
Year of publication	2011
Journal volume	30
Journal issue	24
Pages of publication	6703
a	11.092 ± 0.005 Å
b	15.476 ± 0.006 Å
c	15.867 ± 0.005 Å
α	138.821 ± 0.009°
β	108.491 ± 0.015°
γ	91.926 ± 0.016°
Cell volume	1530.5 ± 1.2 Å³
Cell temperature	203 ± 2 K
Ambient diffraction temperature	203 ± 2 K
Number of distinct elements	5
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0336
Residual factor for significantly intense reflections	0.0279
Weighted residual factors for significantly intense reflections	0.0643
Weighted residual factors for all reflections included in the refinement	0.067
Goodness-of-fit parameter for all reflections included in the refinement	1.048
Diffraction radiation wavelength	0.71069 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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