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Information card for entry 4065546
Preview
Coordinates | 4065546.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C23 H59 Cl Fe N4 Si4 |
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Calculated formula | C23 H59 Cl Fe N4 Si4 |
SMILES | C1=[N+](CCN1C(C)(C)C)C(C)(C)C.C[Si](C)(C)N([Fe](Cl)N([Si](C)(C)C)[Si](C)(C)C)[Si](C)(C)C |
Title of publication | Aminolysis of Bis[bis(trimethylsilyl)amido]iron and -cobalt as a Versatile Route to N-Heterocyclic Carbene Complexes |
Authors of publication | Danopoulos, Andreas A.; Braunstein, Pierre; Stylianides, Neoklis; Wesolek, Marcel |
Journal of publication | Organometallics |
Year of publication | 2011 |
Journal volume | 30 |
Journal issue | 24 |
Pages of publication | 6514 |
a | 17.4562 ± 0.0004 Å |
b | 11.3696 ± 0.0003 Å |
c | 18.4 ± 0.0005 Å |
α | 90° |
β | 102.372 ± 0.001° |
γ | 90° |
Cell volume | 3567.04 ± 0.16 Å3 |
Cell temperature | 120 ± 2 K |
Ambient diffraction temperature | 120 ± 2 K |
Number of distinct elements | 6 |
Space group number | 14 |
Hermann-Mauguin space group symbol | P 1 21/n 1 |
Hall space group symbol | -P 2yn |
Residual factor for all reflections | 0.094 |
Residual factor for significantly intense reflections | 0.0581 |
Weighted residual factors for significantly intense reflections | 0.1011 |
Weighted residual factors for all reflections included in the refinement | 0.116 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.129 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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The link is: https://www.crystallography.net/4065546.html
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