Information card for entry 4065573

Structure parameters

• Formula: C78 H60 B F24 N2 Rh S
• Calculated formula: C78 H60 B F24 N2 Rh S
• Title of publication: Synthesis and Reactions of Coordinatively Unsaturated Half-Sandwich Rhodium and Iridium Complexes Having a 2,6-Dimesitylbenzenethiolate Ligand
• Authors of publication: Sakamoto, Mayumi; Ohki, Yasuhiro; Tatsumi, Kazuyuki
• Journal of publication: Organometallics
• Year of publication: 2010
• Journal volume: 29
• Journal issue: 7
• Pages of publication: 1761
• a: 14.0447 ± 0.0018 Å
• b: 16.641 ± 0.002 Å
• c: 17.788 ± 0.002 Å
• α: 70.042 ± 0.009°
• β: 67.269 ± 0.008°
• γ: 77.022 ± 0.011°
• Cell volume: 3583.5 ± 0.8 ų
• Cell temperature: 173.1 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for significantly intense reflections: 0.046
• Weighted residual factors for all reflections included in the refinement: 0.1292
• Goodness-of-fit parameter for all reflections included in the refinement: 1.026
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No