Information card for entry 4065608

Structure parameters

• Chemical name: catena-(bis(μ~3~-η^2^,η^2^,η^2^-Indenocorannulene)- tris(tetrakis(μ~2~-trifluoroacetato-O,O')-di-rhodium(ii))
• Formula: C42 H12 F24 O16 Rh4
• Calculated formula: C42 H12 F24 O16 Rh4
• Title of publication: Increasing the Curvature of a Bowl-Shaped Polyarene by Fullerene-like η2-Complexation of a Transition Metal at the Interior of the Convex Surface
• Authors of publication: Filatov, Alexander S.; Rogachev, Andrey Yu.; Jackson, Edward A.; Scott, Lawrence T.; Petrukhina, Marina A.
• Journal of publication: Organometallics
• Year of publication: 2010
• Journal volume: 29
• Journal issue: 5
• Pages of publication: 1231
• a: 9.3332 ± 0.0004 Å
• b: 13.0562 ± 0.0006 Å
• c: 21.4259 ± 0.0009 Å
• α: 88.15 ± 0.001°
• β: 77.64 ± 0.001°
• γ: 73.326 ± 0.001°
• Cell volume: 2441.94 ± 0.19 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0552
• Residual factor for significantly intense reflections: 0.0391
• Weighted residual factors for significantly intense reflections: 0.0895
• Weighted residual factors for all reflections included in the refinement: 0.0971
• Goodness-of-fit parameter for all reflections included in the refinement: 1.028
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: Mo-Kα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No