[Bu4P]+Cl−-Catalyzed Reactions of Trichlorosilane and Dichloromethylsilane with Vinyltrichlorosilane: New Synthetic Method for 1,1,4,4-Tetrachloro-2,5-bis(trichlorosilyl)-1,4-disilacyclohexane Compounds
Authors of publication
Hong, Soon Hyun; Hyun, Sang Il; Jung, Il Nam; Han, Won-Sik; Kim, Min-Hye; Yun, Hoseop; Nam, Suk-Woo; Kang, Sang Ook
Journal of publication
Organometallics
Year of publication
2010
Journal volume
29
Journal issue
13
Pages of publication
3054
a
6.1896 ± 0.0005 Å
b
8.3969 ± 0.0007 Å
c
9.0412 ± 0.0009 Å
α
89.363 ± 0.003°
β
80.569 ± 0.003°
γ
78.809 ± 0.002°
Cell volume
454.63 ± 0.07 Å3
Cell temperature
293 ± 2 K
Ambient diffraction temperature
293 ± 2 K
Number of distinct elements
4
Space group number
2
Hermann-Mauguin space group symbol
P -1
Hall space group symbol
-P 1
Residual factor for all reflections
0.0447
Residual factor for significantly intense reflections
0.0394
Weighted residual factors for significantly intense reflections
0.1067
Weighted residual factors for all reflections included in the refinement
0.1103
Goodness-of-fit parameter for all reflections included in the refinement
