Information card for entry 4065648

Structure parameters

• Formula: C27 H32 N6 Ni O4
• Calculated formula: C27 H32 N6 Ni O4
• Title of publication: Chiral Variation of a Hybrid Bis(carbene-amido) Ligand System
• Authors of publication: Jean-Baptiste dit Dominique, François; Gornitzka, Heinz; Hemmert, Catherine
• Journal of publication: Organometallics
• Year of publication: 2010
• Journal volume: 29
• Journal issue: 13
• Pages of publication: 2868
• a: 14.7743 ± 0.001 Å
• b: 16.0012 ± 0.001 Å
• c: 12.3916 ± 0.0009 Å
• α: 90°
• β: 112.797 ± 0.004°
• γ: 90°
• Cell volume: 2700.6 ± 0.3 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 5
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0836
• Residual factor for significantly intense reflections: 0.0443
• Weighted residual factors for significantly intense reflections: 0.0762
• Weighted residual factors for all reflections included in the refinement: 0.0884
• Goodness-of-fit parameter for all reflections included in the refinement: 1.004
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No