Information card for entry 4065657

Structure parameters

• Formula: C66 H92 Fe2 N2
• Calculated formula: C66 H92 Fe2 N2
• Title of publication: Reaction of M(II) Diaryls (M = Mn or Fe) with Ammonia to Afford Parent Amido Complexes
• Authors of publication: Ni, Chengbao; Lei, Hao; Power, Philip P.
• Journal of publication: Organometallics
• Year of publication: 2010
• Journal volume: 29
• Journal issue: 8
• Pages of publication: 1988
• a: 11.963 ± 0.002 Å
• b: 20.35 ± 0.003 Å
• c: 12.583 ± 0.002 Å
• α: 90°
• β: 99.002 ± 0.002°
• γ: 90°
• Cell volume: 3025.6 ± 0.8 ų
• Cell temperature: 90 ± 2 K
• Ambient diffraction temperature: 90 ± 2 K
• Number of distinct elements: 4
• Space group number: 12
• Hermann-Mauguin space group symbol: I 1 2/m 1
• Hall space group symbol: -I 2y
• Residual factor for all reflections: 0.0545
• Residual factor for significantly intense reflections: 0.0434
• Weighted residual factors for significantly intense reflections: 0.1158
• Weighted residual factors for all reflections included in the refinement: 0.124
• Goodness-of-fit parameter for all reflections included in the refinement: 1.087
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No