Information card for entry 4065682

Structure parameters

• Formula: C50 H53 Cl7 O5 P2 Rh2
• Calculated formula: C50 H53 Cl7 O5 P2 Rh2
• Title of publication: Synthesis of Oxygen- and Sulfur-Bridged Dirhodium Complexes and Their Use As Catalysts in the Chemoselective Hydrogenation of Alkenes
• Authors of publication: Zhu, Chuan; Yukimura, Noriaki; Yamane, Motoki
• Journal of publication: Organometallics
• Year of publication: 2010
• Journal volume: 29
• Journal issue: 9
• Pages of publication: 2098
• a: 13.389 ± 0.004 Å
• b: 13.783 ± 0.004 Å
• c: 14.458 ± 0.004 Å
• α: 79.908 ± 0.008°
• β: 79.935 ± 0.008°
• γ: 80.945 ± 0.008°
• Cell volume: 2564.2 ± 1.3 ų
• Cell temperature: 120 ± 2 K
• Ambient diffraction temperature: 120 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0357
• Residual factor for significantly intense reflections: 0.0308
• Weighted residual factors for significantly intense reflections: 0.0751
• Weighted residual factors for all reflections included in the refinement: 0.0789
• Goodness-of-fit parameter for all reflections included in the refinement: 1.037
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No