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Information card for entry 4065689
Preview
Coordinates | 4065689.cif |
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Original paper (by DOI) | HTML |
Formula | C42 H55 N3 U |
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Calculated formula | C42 H55 N3 U |
Title of publication | Utility of the 1,3,4,6,7,8-Hexahydro-2H-pyrimido[1,2-a]pyrimidinato Ligand, (hpp)−, in Stabilizing Uranium Metallocene Mono-Alkyl and “Tuck-in” Complexes |
Authors of publication | Montalvo, Elizabeth; Ziller, Joseph W.; DiPasquale, Antonio G.; Rheingold, Arnold L.; Evans, William J. |
Journal of publication | Organometallics |
Year of publication | 2010 |
Journal volume | 29 |
Journal issue | 9 |
Pages of publication | 2104 |
a | 10.4092 ± 0.0011 Å |
b | 10.3444 ± 0.0011 Å |
c | 34.255 ± 0.004 Å |
α | 90° |
β | 91.4437 ± 0.0013° |
γ | 90° |
Cell volume | 3687.3 ± 0.7 Å3 |
Cell temperature | 153 ± 2 K |
Ambient diffraction temperature | 153 ± 2 K |
Number of distinct elements | 4 |
Space group number | 14 |
Hermann-Mauguin space group symbol | P 1 21/n 1 |
Hall space group symbol | -P 2yn |
Residual factor for all reflections | 0.0512 |
Residual factor for significantly intense reflections | 0.0476 |
Weighted residual factors for significantly intense reflections | 0.0991 |
Weighted residual factors for all reflections included in the refinement | 0.1003 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.341 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/4065689.html
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Users of the data should acknowledge the original authors of the
structural data.