Information card for entry 4065734

Structure parameters

• Formula: C90 H110 Dy2 I2 N4 O P4 Si4
• Calculated formula: C76 H94 Dy2 I2 N4 O P4 Si4
• SMILES: C12=P(c3ccccc3)(c3ccccc3)N([Dy]2(I)([N](=P1(c1ccccc1)c1ccccc1)[Si](C)(C)C)O[Dy]12(C(=P(c3ccccc3)(c3ccccc3)N1[Si](C)(C)C)P(=[N]2[Si](C)(C)C)(c1ccccc1)c1ccccc1)I)[Si](C)(C)C.Cc1ccccc1.Cc1ccccc1
• Title of publication: Synthesis and Characterization of Dysprosium and Lanthanum Bis(iminophosphorano)methanide and -methanediide Complexes
• Authors of publication: Wooles, Ashley J.; Cooper, Oliver J.; McMaster, Jonathan; Lewis, William; Blake, Alexander J.; Liddle, Stephen T.
• Journal of publication: Organometallics
• Year of publication: 2010
• Journal volume: 29
• Journal issue: 10
• Pages of publication: 2315
• a: 12.181 ± 0.0008 Å
• b: 13.0289 ± 0.0009 Å
• c: 15.692 ± 0.001 Å
• α: 97.652 ± 0.002°
• β: 92.036 ± 0.002°
• γ: 105.32 ± 0.002°
• Cell volume: 2374 ± 0.3 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 8
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0351
• Residual factor for significantly intense reflections: 0.0311
• Weighted residual factors for significantly intense reflections: 0.0827
• Weighted residual factors for all reflections included in the refinement: 0.0848
• Goodness-of-fit parameter for all reflections included in the refinement: 1.063
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No