Crystallography Open Database

Information card for entry 4065742

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Coordinates	4065742.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C33 H60 Cl F P2 Rh
Calculated formula	C33 H60 Cl F P2 Rh
Title of publication	C−C Bond Activation of a Cyclopropyl Phosphine: Isolation and Reactivity of a Tetrameric Rhodacyclobutane
Authors of publication	Chaplin, Adrian B.; Weller, Andrew S.
Journal of publication	Organometallics
Year of publication	2010
Journal volume	29
Journal issue	10
Pages of publication	2332
a	20.1059 ± 0.0002 Å
b	13.0009 ± 0.0002 Å
c	26.4447 ± 0.0004 Å
α	90°
β	92.2748 ± 0.0005°
γ	90°
Cell volume	6907.06 ± 0.16 Å³
Cell temperature	150 ± 2 K
Ambient diffraction temperature	150 ± 2 K
Number of distinct elements	6
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.0446
Residual factor for significantly intense reflections	0.0314
Weighted residual factors for significantly intense reflections	0.0634
Weighted residual factors for all reflections included in the refinement	0.0685
Goodness-of-fit parameter for all reflections included in the refinement	1.029
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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