Crystallography Open Database
- COD Home
- Accessing COD Data
- Add Your Data
- Documentation
Information card for entry 4065752
Preview
Coordinates | 4065752.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C78 H70 Cl6 Ge2 O2 |
---|---|
Calculated formula | C78 H70 Cl6 Ge2 O2 |
Title of publication | Reactions of Germenes with Somepara-Quinones: Formation of a Tricyclic Compound from 1,4-Benzoquinone Undergoing an Unexpected Rearrangement† |
Authors of publication | Ghereg, Dumitru; André, Erwan; Ech-Cherif El Kettani, Sakina; Saffon, Nathalie; Lazraq, Mohamed; Ranaivonjatovo, Henri; Gornitzka, Heinz; Miqueu, Karinne; Sotiropoulos, Jean-Marc; Escudié, Jean |
Journal of publication | Organometallics |
Year of publication | 2010 |
Journal volume | 29 |
Journal issue | 21 |
Pages of publication | 4849 |
a | 11.0136 ± 0.0017 Å |
b | 16.376 ± 0.003 Å |
c | 20.416 ± 0.003 Å |
α | 67.051 ± 0.003° |
β | 89.171 ± 0.003° |
γ | 85.84 ± 0.003° |
Cell volume | 3381.4 ± 1 Å3 |
Cell temperature | 173 ± 2 K |
Ambient diffraction temperature | 173 ± 2 K |
Number of distinct elements | 5 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.0854 |
Residual factor for significantly intense reflections | 0.0481 |
Weighted residual factors for significantly intense reflections | 0.102 |
Weighted residual factors for all reflections included in the refinement | 0.1162 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.016 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/4065752.html
All data in the COD and the database itself are dedicated to the
public domain and licensed under the
CC0
License
.
Users of the data should acknowledge the original authors of the
structural data.