Information card for entry 4065761

Structure parameters

• Formula: C42 H74 N2 O P4 Pb2 S4
• Calculated formula: C42 H74 N2 O P4 Pb2 S4
• SMILES: [Pb]12[n]3c(cccc3CP(=S)(C(C)C)C(C)C)C1([Pb]1[n]3c(cccc3CP(=S)(C(C)C)C(C)C)C21P(=S)(C(C)C)C(C)C)P(=S)(C(C)C)C(C)C.C1CCCO1
• Title of publication: Synthesis of Heavier Group 14 Metal Compounds from 2,6-Lutidylbis(phosphoranosulfide)
• Authors of publication: Leung, Wing-Por; Kan, Kwok-Wai; Mak, Thomas C. W.
• Journal of publication: Organometallics
• Year of publication: 2010
• Journal volume: 29
• Journal issue: 8
• Pages of publication: 1890
• a: 10.533 ± 0.003 Å
• b: 15.395 ± 0.004 Å
• c: 16.602 ± 0.004 Å
• α: 78.485 ± 0.005°
• β: 85.666 ± 0.005°
• γ: 85.908 ± 0.006°
• Cell volume: 2626 ± 1.2 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0561
• Residual factor for significantly intense reflections: 0.0428
• Weighted residual factors for significantly intense reflections: 0.1113
• Weighted residual factors for all reflections included in the refinement: 0.1198
• Goodness-of-fit parameter for all reflections included in the refinement: 1.027
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No