Information card for entry 4065863

Structure parameters

• Formula: C31.5 H17 F16 N4 O2 P2 Rh
• Calculated formula: C31.5 H17 F16 N4 O2 P2 Rh
• Title of publication: Reaction of Secondary Phosphine Oxides with Rhodium(I)
• Authors of publication: Christiansen, Andrea; Selent, Detlef; Spannenberg, Anke; Baumann, Wolfgang; Franke, Robert; Börner, Armin
• Journal of publication: Organometallics
• Year of publication: 2010
• Journal volume: 29
• Journal issue: 14
• Pages of publication: 3139
• a: 13.8014 ± 0.0005 Å
• b: 15.818 ± 0.0007 Å
• c: 15.8529 ± 0.0006 Å
• α: 90°
• β: 90.31 ± 0.003°
• γ: 90°
• Cell volume: 3460.8 ± 0.2 ų
• Cell temperature: 200 ± 2 K
• Ambient diffraction temperature: 200 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0357
• Residual factor for significantly intense reflections: 0.026
• Weighted residual factors for significantly intense reflections: 0.0608
• Weighted residual factors for all reflections included in the refinement: 0.0626
• Goodness-of-fit parameter for all reflections included in the refinement: 0.939
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No