Information card for entry 4065893

Structure parameters

• Formula: C23 H21 Cl F6 N7 Os P
• Calculated formula: C23 H21 Cl F6 N7 Os P
• Title of publication: Osmium Complexes Containing N-Heterocyclic Carbene-Based C,N,C-Pincer Ligands
• Authors of publication: Wong, Chun-Yuen; Lai, Lo-Ming; Pat, Pak-Kei; Chung, Lai-Hon
• Journal of publication: Organometallics
• Year of publication: 2010
• Journal volume: 29
• Journal issue: 11
• Pages of publication: 2533
• a: 14.7557 ± 0.0002 Å
• b: 13.193 ± 0.0002 Å
• c: 14.9139 ± 0.0002 Å
• α: 90°
• β: 93.475 ± 0.001°
• γ: 90°
• Cell volume: 2897.98 ± 0.07 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0304
• Residual factor for significantly intense reflections: 0.0241
• Weighted residual factors for significantly intense reflections: 0.0587
• Weighted residual factors for all reflections included in the refinement: 0.0602
• Goodness-of-fit parameter for all reflections included in the refinement: 1.012
• Diffraction radiation wavelength: 1.54178 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No