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Information card for entry 4065921
Preview
Coordinates | 4065921.cif |
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Original paper (by DOI) | HTML |
Formula | C24 H54 Cl2 P2 Ru Si |
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Calculated formula | C24 H54 Cl2 P2 Ru Si |
Title of publication | C−H Bond Activation of Terminal Allenes: Formation of Hydride-Alkenylcarbyne-Osmium and Disubstituted Vinylidene-Ruthenium Derivativesā„ |
Authors of publication | Collado, Alba; Esteruelas, Miguel A.; López, Fernando; Mascareñas, José L.; Oñate, Enrique; Trillo, Beatriz |
Journal of publication | Organometallics |
Year of publication | 2010 |
Journal volume | 29 |
Journal issue | 21 |
Pages of publication | 4966 |
a | 19.498 ± 0.007 Å |
b | 12.003 ± 0.004 Å |
c | 15.441 ± 0.006 Å |
α | 90° |
β | 120.064 ± 0.006° |
γ | 90° |
Cell volume | 3128 ± 2 Å3 |
Cell temperature | 100 ± 2 K |
Ambient diffraction temperature | 100 ± 2 K |
Number of distinct elements | 6 |
Space group number | 15 |
Hermann-Mauguin space group symbol | C 1 2/c 1 |
Hall space group symbol | -C 2yc |
Residual factor for all reflections | 0.0696 |
Residual factor for significantly intense reflections | 0.0449 |
Weighted residual factors for significantly intense reflections | 0.0855 |
Weighted residual factors for all reflections included in the refinement | 0.0937 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.034 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/4065921.html
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