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Information card for entry 4065942
Preview
Coordinates | 4065942.cif |
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Original paper (by DOI) | HTML |
Formula | C68 H56 B D6 F15 Hf2 |
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Calculated formula | C68 H62 B F15 Hf2 |
Title of publication | Reactions of the Five-Membered Hafnacyclocumulene Cp2Hf(η4-t-Bu-C4-t-Bu) with the Lewis Acids Tris(pentafluorophenyl)borane and Diisobutylaluminum Hydride |
Authors of publication | Burlakov, Vladimir V.; Beweries, Torsten; Kaleta, Katharina; Bogdanov, Vyacheslav S.; Arndt, Perdita; Baumann, Wolfgang; Spannenberg, Anke; Shur, Vladimir B.; Rosenthal, Uwe |
Journal of publication | Organometallics |
Year of publication | 2010 |
Journal volume | 29 |
Journal issue | 10 |
Pages of publication | 2367 |
a | 10.1365 ± 0.0003 Å |
b | 15.8667 ± 0.0005 Å |
c | 19.3646 ± 0.0006 Å |
α | 83.164 ± 0.003° |
β | 76.599 ± 0.003° |
γ | 89.156 ± 0.003° |
Cell volume | 3007.86 ± 0.17 Å3 |
Cell temperature | 200 ± 2 K |
Ambient diffraction temperature | 200 ± 2 K |
Number of distinct elements | 6 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.0405 |
Residual factor for significantly intense reflections | 0.0245 |
Weighted residual factors for significantly intense reflections | 0.0433 |
Weighted residual factors for all reflections included in the refinement | 0.0452 |
Goodness-of-fit parameter for all reflections included in the refinement | 0.941 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/4065942.html
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Users of the data should acknowledge the original authors of the
structural data.