Information card for entry 4065977

Structure parameters

• Formula: C47 H69 Ge O P
• Calculated formula: C47 H69 Ge O P
• Title of publication: The Reactivity of Phosphagermaallene Mes*P═C═Ge(t-Bu)Tip toward Aldehydes and Ketones: an Experimental and Theoretical Study
• Authors of publication: Ouhsaine, F.; André, E.; Sotiropoulos, J. M.; Escudié, J.; Ranaivonjatovo, H.; Gornitzka, H.; Saffon, N.; Miqueu, K.; Lazraq, M.
• Journal of publication: Organometallics
• Year of publication: 2010
• Journal volume: 29
• Journal issue: 11
• Pages of publication: 2566
• a: 37.647 ± 0.014 Å
• b: 9.876 ± 0.004 Å
• c: 29.559 ± 0.017 Å
• α: 90°
• β: 127.753 ± 0.004°
• γ: 90°
• Cell volume: 8689 ± 7 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 5
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.1528
• Residual factor for significantly intense reflections: 0.125
• Weighted residual factors for significantly intense reflections: 0.2576
• Weighted residual factors for all reflections included in the refinement: 0.269
• Goodness-of-fit parameter for all reflections included in the refinement: 1.235
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No