Crystallography Open Database

Information card for entry 4066028

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Coordinates	4066028.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C36 H53 Li N3 Nb O2
Calculated formula	C36 H53 Li N3 Nb O2
Title of publication	Synthesis, Characterization, and Reactions of Isolable (β-Diketiminato)Nb(III) Imido Complexes.
Authors of publication	Tomson, Neil C.; Arnold, John; Bergman, Robert G.
Journal of publication	Organometallics
Year of publication	2010
Journal volume	29
Journal issue	21
Pages of publication	5010 - 5025
a	11.4341 ± 0.0005 Å
b	12.9987 ± 0.0006 Å
c	14.2141 ± 0.0007 Å
α	73.069 ± 0.001°
β	85.136 ± 0.001°
γ	74.461 ± 0.001°
Cell volume	1947.13 ± 0.16 Å³
Cell temperature	141 ± 2 K
Ambient diffraction temperature	141 ± 2 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0638
Residual factor for significantly intense reflections	0.0485
Weighted residual factors for significantly intense reflections	0.1134
Weighted residual factors for all reflections included in the refinement	0.1206
Goodness-of-fit parameter for all reflections included in the refinement	1.063
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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