Information card for entry 4066032

Structure parameters

• Formula: C35.25 H50.25 Cl Pt S3 Si
• Calculated formula: C35.25 H45 Cl Pt S3 Si
• Title of publication: Synthesis and Complexation of a New Tripodal Tetradentate Ligand, a Silyl Ligand Tethered with Three Thioether Moieties
• Authors of publication: Takeda, Nobuhiro; Watanabe, Daisuke; Nakamura, Tetsu; Unno, Masafumi
• Journal of publication: Organometallics
• Year of publication: 2010
• Journal volume: 29
• Journal issue: 13
• Pages of publication: 2839
• a: 11.1478 ± 0.0008 Å
• b: 18.9318 ± 0.0017 Å
• c: 19.6732 ± 0.0017 Å
• α: 109.292 ± 0.002°
• β: 100.757 ± 0.0019°
• γ: 97.736 ± 0.0018°
• Cell volume: 3762.7 ± 0.5 ų
• Cell temperature: 123 ± 2 K
• Ambient diffraction temperature: 123 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0719
• Residual factor for significantly intense reflections: 0.0692
• Weighted residual factors for significantly intense reflections: 0.1286
• Weighted residual factors for all reflections included in the refinement: 0.1296
• Goodness-of-fit parameter for all reflections included in the refinement: 1.327
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No