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Information card for entry 4066076
Preview
Coordinates | 4066076.cif |
---|---|
Original paper (by DOI) | HTML |
Common name | eisjz03 |
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Formula | C40 H46 Cl10 N2 O2 P2 Pd |
Calculated formula | C40 H46 Cl10 N2 O2 P2 Pd |
SMILES | [Pd]1(Cl)(Cl)[P@]2(CC[P@@]31OC([C@H]1N3CCC1)(c1ccccc1)c1ccccc1)OC([C@H]1N2CCC1)(c1ccccc1)c1ccccc1.C(Cl)Cl.C(Cl)Cl.C(Cl)Cl.C(Cl)Cl |
Title of publication | Dicationic Palladium(II) Complexes as Active Lewis Acid Catalysts for Polarized Nazarov Cyclization |
Authors of publication | Zhang, Jing; Vaidya, Tulaza; Brennessel, William W.; Frontier, Alison J.; Eisenberg, Richard |
Journal of publication | Organometallics |
Year of publication | 2010 |
Journal volume | 29 |
Journal issue | 15 |
Pages of publication | 3341 |
a | 19.357 ± 0.003 Å |
b | 22.915 ± 0.003 Å |
c | 31.461 ± 0.004 Å |
α | 90° |
β | 90° |
γ | 90° |
Cell volume | 13955 ± 3 Å3 |
Cell temperature | 100 ± 0.1 K |
Ambient diffraction temperature | 100 ± 0.1 K |
Number of distinct elements | 7 |
Space group number | 19 |
Hermann-Mauguin space group symbol | P 21 21 21 |
Hall space group symbol | P 2ac 2ab |
Residual factor for all reflections | 0.1179 |
Residual factor for significantly intense reflections | 0.0697 |
Weighted residual factors for significantly intense reflections | 0.1517 |
Weighted residual factors for all reflections included in the refinement | 0.1764 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.009 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/4066076.html
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