Information card for entry 4066081

Structure parameters

• Formula: C24 H56 P8 Pd2
• Calculated formula: C24 H56 P8 Pd2
• Title of publication: Preparation and Thermal Reaction of Tetrastannapalladacyclopentane. Sn−Sn Bond Formation and Cleavage
• Authors of publication: Tanabe, Makoto; Hanzawa, Masaya; Osakada, Kohtaro
• Journal of publication: Organometallics
• Year of publication: 2010
• Journal volume: 29
• Journal issue: 16
• Pages of publication: 3535
• a: 11.778 ± 0.003 Å
• b: 11.869 ± 0.003 Å
• c: 14.363 ± 0.003 Å
• α: 90°
• β: 92.983 ± 0.003°
• γ: 90°
• Cell volume: 2005.1 ± 0.8 ų
• Cell temperature: 113.1 K
• Ambient diffraction temperature: 113 ± 2 K
• Number of distinct elements: 4
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0366
• Residual factor for significantly intense reflections: 0.0344
• Weighted residual factors for significantly intense reflections: 0.0947
• Weighted residual factors for all reflections included in the refinement: 0.0966
• Goodness-of-fit parameter for all reflections included in the refinement: 1.027
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No