Information card for entry 4066084

Structure parameters

• Formula: C56 H69 N4 O4 Yb
• Calculated formula: C55.96 H61 N4 O3.99 Yb
• Title of publication: Quinoline Ring C−H Bond Activation in Bis(3,5-di-tert-butylsalicylidene)-8-aminoquinoline Bis(trimethylsilyl)amido Lanthanide Complexes
• Authors of publication: Han, Fubin; Li, Bangyu; Zhang, Yong; Wang, Yaorong; Shen, Qi
• Journal of publication: Organometallics
• Year of publication: 2010
• Journal volume: 29
• Journal issue: 15
• Pages of publication: 3467
• a: 14.012 ± 0.002 Å
• b: 17.642 ± 0.003 Å
• c: 22.742 ± 0.003 Å
• α: 90°
• β: 103.347 ± 0.003°
• γ: 90°
• Cell volume: 5470 ± 1.4 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0735
• Residual factor for significantly intense reflections: 0.0624
• Weighted residual factors for significantly intense reflections: 0.1384
• Weighted residual factors for all reflections included in the refinement: 0.1448
• Goodness-of-fit parameter for all reflections included in the refinement: 1.152
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No