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Information card for entry 4066090
Preview
Coordinates | 4066090.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C18 H37 N O2 Si2 W |
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Calculated formula | C18 H37 N O2 Si2 W |
SMILES | C(N1O[W]23451(C[Si](C)(C)C)([c]1([c]5([c]4([c]3([c]21C)C)C)C)C)=O)[Si](C)(C)C |
Title of publication | Hydroperoxide-Initiated Intramolecular Insertions of NO into Metal−Carbon Bonds† |
Authors of publication | Graham, Peter M.; Buschhaus, Miriam S. A.; Baillie, Rhett A.; Semproni, Scott P.; Legzdins, Peter |
Journal of publication | Organometallics |
Year of publication | 2010 |
Journal volume | 29 |
Journal issue | 21 |
Pages of publication | 5068 |
a | 9.9833 ± 0.0009 Å |
b | 10.6781 ± 0.001 Å |
c | 12.7497 ± 0.0011 Å |
α | 110.998 ± 0.004° |
β | 111.235 ± 0.004° |
γ | 95.911 ± 0.004° |
Cell volume | 1139.64 ± 0.19 Å3 |
Cell temperature | 173 ± 2 K |
Ambient diffraction temperature | 173 ± 2 K |
Number of distinct elements | 6 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.0184 |
Residual factor for significantly intense reflections | 0.0172 |
Weighted residual factors for significantly intense reflections | 0.0408 |
Weighted residual factors for all reflections included in the refinement | 0.0412 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.121 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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