Information card for entry 4066119

Structure parameters

• Chemical name: 1-(2,6-dimesitylphenyl)-1,3-di(tert-butyl)-3-trimethylsilyl-1-sila-allene benzene solvate (2:1)
• Formula: C80 H110 Si4
• Calculated formula: C80 H110 Si4
• Title of publication: Formation of a Silylated 1-Silaallene via an Intermediate 1-Chloro-1-silaallene
• Authors of publication: Spirk, Stefan; Belaj, Ferdinand; Albering, Jörg H.; Pietschnig, Rudolf
• Journal of publication: Organometallics
• Year of publication: 2010
• Journal volume: 29
• Journal issue: 13
• Pages of publication: 2981
• a: 11.89 ± 0.0009 Å
• b: 13.6503 ± 0.0009 Å
• c: 23.2007 ± 0.0016 Å
• α: 102.985 ± 0.003°
• β: 104.076 ± 0.003°
• γ: 90.135 ± 0.003°
• Cell volume: 3552.6 ± 0.4 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 3
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0656
• Residual factor for significantly intense reflections: 0.0578
• Weighted residual factors for significantly intense reflections: 0.1375
• Weighted residual factors for all reflections included in the refinement: 0.1425
• Goodness-of-fit parameter for all reflections included in the refinement: 1.087
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No