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Information card for entry 4066196
Preview
Coordinates | 4066196.cif |
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Original paper (by DOI) | HTML |
Formula | C22 H27 Fe2 N2 O4 P |
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Calculated formula | C22 H27 Fe2 N2 O4 P |
Title of publication | Reactions of the Phosphinidene-Bridged Complexes [Fe2(η5-C5H5)2(μ-PR)(μ-CO)(CO)2] (R = Cy, Ph, 2,4,6-C6H2tBu3) with Diazoalkanes. Formation and Rearrangements of Phosphadiazadiene-Bridged Derivatives† |
Authors of publication | Alvarez, M. Angeles; García, M. Esther; González, Rocío; Ruiz, Miguel A. |
Journal of publication | Organometallics |
Year of publication | 2010 |
Journal volume | 29 |
Journal issue | 21 |
Pages of publication | 5140 |
a | 11.0876 ± 0.0003 Å |
b | 13.7702 ± 0.0004 Å |
c | 15.7119 ± 0.0005 Å |
α | 72.167 ± 0.002° |
β | 72.183 ± 0.002° |
γ | 77.026 ± 0.002° |
Cell volume | 2151.32 ± 0.11 Å3 |
Cell temperature | 100 ± 0.1 K |
Ambient diffraction temperature | 100 ± 0.1 K |
Number of distinct elements | 6 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.0956 |
Residual factor for significantly intense reflections | 0.0548 |
Weighted residual factors for significantly intense reflections | 0.1372 |
Weighted residual factors for all reflections included in the refinement | 0.1523 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.078 |
Diffraction radiation probe | x-ray |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
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