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Information card for entry 4066223
Preview
Coordinates | 4066223.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C60 H98 Al2 Ge Si8 |
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Calculated formula | C60 H98 Al2 Ge Si8 |
Title of publication | Facile Synthesis of an Unsaturated Spiro Germane by Hydroalumination and Intramolecular 1,1-Carbalumination† |
Authors of publication | Uhl, Werner; Rohling, Martina; Würthwein, Ernst-Ulrich; Ghavtadze, Nugzar; Bergander, Klaus |
Journal of publication | Organometallics |
Year of publication | 2010 |
Journal volume | 29 |
Journal issue | 21 |
Pages of publication | 5236 |
a | 14.9993 ± 0.0005 Å |
b | 21.4156 ± 0.0007 Å |
c | 22.9117 ± 0.0008 Å |
α | 80.823 ± 0.001° |
β | 74.138 ± 0.001° |
γ | 80.236 ± 0.001° |
Cell volume | 6927 ± 0.4 Å3 |
Cell temperature | 153 ± 2 K |
Ambient diffraction temperature | 153 ± 2 K |
Number of distinct elements | 5 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.0914 |
Residual factor for significantly intense reflections | 0.0485 |
Weighted residual factors for significantly intense reflections | 0.1064 |
Weighted residual factors for all reflections included in the refinement | 0.1223 |
Goodness-of-fit parameter for all reflections included in the refinement | 0.976 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/4066223.html
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