Information card for entry 4066223

Structure parameters

• Formula: C60 H98 Al2 Ge Si8
• Calculated formula: C60 H98 Al2 Ge Si8
• Title of publication: Facile Synthesis of an Unsaturated Spiro Germane by Hydroalumination and Intramolecular 1,1-Carbalumination†
• Authors of publication: Uhl, Werner; Rohling, Martina; Würthwein, Ernst-Ulrich; Ghavtadze, Nugzar; Bergander, Klaus
• Journal of publication: Organometallics
• Year of publication: 2010
• Journal volume: 29
• Journal issue: 21
• Pages of publication: 5236
• a: 14.9993 ± 0.0005 Å
• b: 21.4156 ± 0.0007 Å
• c: 22.9117 ± 0.0008 Å
• α: 80.823 ± 0.001°
• β: 74.138 ± 0.001°
• γ: 80.236 ± 0.001°
• Cell volume: 6927 ± 0.4 ų
• Cell temperature: 153 ± 2 K
• Ambient diffraction temperature: 153 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0914
• Residual factor for significantly intense reflections: 0.0485
• Weighted residual factors for significantly intense reflections: 0.1064
• Weighted residual factors for all reflections included in the refinement: 0.1223
• Goodness-of-fit parameter for all reflections included in the refinement: 0.976
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No